MS Report from Instrument: HY-LCMS-02 File ..HEM32\\1\\DATA\\20170117\\BIZ\\BIZ2017-117-WJ1.D Tgt Mass (EZX): 427.00 Injection Date : 17 Jan 17 9:21 am +0800 Seq. Line : 0 Sample Name : BIZ2017-117-WJ1 Location : P1-A-06 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\Chem32\\1\\METHODS\\1-STANDBY.M Catalog No : HY-D0098 Batch#23299 Easy-Access Method: '1-POS-3MIN' 427.00 Method Info : Column: A-RP-169 *DAD1 B, Sig=214,4 Ref=off mAU100050000.5*DAD1 C, Sig=2,4 Ref=off mAU10011..5502211.5751.7492.1185000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70100000800006000040000200000.51 Ion 428, MSD1 428,Target Mass 427 +H Positive, EIC=427.7:428.7 1.51.59922.5min1.59911.62211..5502211.5561.5971.7491.51.62222.5min*1.522.5min*400002000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.50 0.02 6.80 7.77 0.44 348 1.52 0.02 16.16 14.74 1.05 309 1.56 0.02 1.70 0.23 0.11 428 1.60 0.02 0.77 2.18 0.05 428 1.62 0.02 1510.71 1352.02 98.00 428 1.75 0.02 5.37 5.57 0.35 233 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.50 0.02 2.13 2.28 1.11 229 1.52 0.02 3.66 3.42 1.91 309 1.57 0.03 0.40 0.38 0.21 428 1.62 0.02 182.47 162.18 95.29 428 1.75 0.02 1.55 1.59 0.81 233 2.12 0.02 1.28 1.30 0.67 233HY-LCMS-02 1/18/2017 12:58:24 PM GZZ_718Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.60 <<<< POSITIVE SPECTRA >>>> ES-API Positive25000200001500010000 229.250000200300400500600700800900m/z 309.2 430.1 429.1 428.1HY-LCMS-02 1/18/2017 12:58:24 PM GZZ_718Page 2 of 2
