MS Report from Instrument: LCMS-03 File ..3\\Data\\20180120\\20180120\\BIZ2018-120-WYQ5.D Tgt Mass (CHM): Injection Date : 20 Jan 18 3:34 pm +0800 Seq. Line : 82 Sample Name : BIZ2018-120-WYQ5 Location : P2-A-07 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 2 ul Acq. Method : D:\\LCMS03\\Data\\20180120\\20180120\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20180120\\20180120\\1-POS-3MIN.M Catalog No : HY-111285 Batch#28341 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=offmAU1000000.5 DAD1 B, Sig=254,4 Ref=offmAU200000.5 ELS1 A, ELSD SignalmV5000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7020000001000000min1.51.81522.5min11.51.85611.4711.87420001.7891.51.78922.5min1.8742.02922.5min00.51 Ion 264, MSD1 264,Target Mass 263 +H Positive, EIC=263.7:264.7600000400000200000000.511.51.81422.51.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.47 0.02 4.08 3.45 0.28 157 1.79 0.02 1036.73 913.07 71.78 264 1.87 0.02 403.52 342.55 27.94 264 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.79 0.02 582.03 508.74 88.50 264 1.87 0.02 74.76 64.97 11.37 264 2.03 0.02 0.87 0.74 0.13 157 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.82 0.06 4434636.00 1213398.38 100.00 264LCMS-03 1/22/2018 10:49:11 AM SYSTEMPage1 of3MS Report from Instrument: LCMS-03Ret. Time: 1.82 <<<< POSITIVE SPECTRA >>>> ES-API Positive264.11750001500001250001000007500050000250000100200300400500600700800900m/z159.1179.1105.1265.1157.1286.1549.2LCMS-03 1/22/2018 10:49:11 AM SYSTEMPage2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 1/22/2018 10:49:11 AM SYSTEMPage3 of3
