MS Report from Instrument: LCMS-03 File ..ata\\20171102\\20171102-1\\BIZ2017-N02-WYQ14.D Tgt Mass (CHM): Injection Date : 2 Nov 17 1:42 pm +0800 Seq. Line : 20 Sample Name : BIZ2017-N02-WYQ14 Location : P1-E-03 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171102\\20171102-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171102\\20171102-1\\1-POS-3MIN.M Catalog No : HY-B0604 Batch#27027 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off0.276mAU500000.5 DAD1 B, Sig=2,4 Ref=off0.276mAU1000000.5 ELS1 A, ELSD Signal0.341mV402000.511.5 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70 **** NO MS PEAKS INTEGRATED ****750000500000250000000.51 Ion 95, MSD1 95,Target Mass 94 +H Positive, EIC=94.7:95.70.050-0.05-0.100.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.522.5min22.5min111.522.1112.12.5min11..3335361.6171.9222.1111.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.28 0.02 1500.91 1261.74 99.97 135 2.11 0.01 0.27 0.39 0.02 105 2.15 0.01 0.20 0.01 0.01 105 Integration Results for DAD1 B, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.28 0.02 2822.78 2306.06 99. 135 1.33 0.02 1.41 1.34 0.05 135 1.36 0.01 0.68 0.77 0.02 135 1.62 0.02 0.44 0.40 0.02 135 1.92 0.02 0.30 0.02 0.01 233 2.11 0.01 0.23 0.31 0.01 105 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|LCMS-03 11/2/2017 14:02:44 SYSTEMPage1 of2MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 11/2/2017 14:02:44 SYSTEMPage2 of2
